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Skip directly to search Skip directly to A to Z list Skip directly to page options Skip directly to site content. An analytical method was developed for the determination of 1-chloro- 1-nitropropane in airborne samples. The protocol consisted of the analysis of 18 spiked samples containing 50, , and percent of the OSHA standard of 20 parts per million and 18 dynamically generated samples with the same volume. Precision and accuracy of the method and storage stability of the samples were assessed. A known volume of air was drawn through a tube containing Chromosorb , which was then transferred to vials and the 1-chloro- 1-nitropropane was desorbed with ethyl-acetate. Aliquots of solution were then injected into gas chromatograph with a flame ionization detector.
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